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Metallorganic Molecular Beam Epitaxy (MOMBE)

Principal Investigator: Dr. Cammy Abernathy

Molecular Beam Epitaxy (MBE) of III-V compound semiconductors is carried out in a modified Varian Gen II (MOD Gen II) growth system. The MBE technique allows individual atomic layers to be deposited one layer at a time in the controlled high vacuum (~5 X 10-9 torr) environment of the central growth chamber. The system is configured to enable both gas source molecular beam epitaxy (GSMBE) and metallorganic molecular beam epitaxy (MOMBE) of Group III nitrides, phosphides, arsenides, and antimonides. The system can accommodate up to six metallorganic or dopant bubbler sources, such as triethylgallium, trimethylgallium, trimethylindium, dimethylethylamine alane, silicon tetrabromide, carbon tetrabromide, or biscyclopentadienylmagnesium. The bubbler source materials are introduced into the growth chamber by an injector head via a sophisticated gas delivery system, controlled from a PC running LabviewÔ control software. Recirculating temperature baths are also used to control the bubbler temperatures during growth. The system also contains four shuttered effusion cells to enable standard solid source MBE growth of III-V materials. These cells in the past have been used to provide atomic beams of Ga, In, Sb, Mn, Eu, Er, and Tl. A high temperature thermal cracker for hydrides attached to the system provides atomic beams of P and As from bottles of PH3 and AsH3. Finally, atomic nitrogen in provided by a separate RF cracker unit. Samples are manipulated by way of a magnetic trolley system that can move up to sixteen separate sample blocks at one time from the system load lock to the growth chamber by way of an intermediary high vacuum buffer chamber. The sample blocks are removed from the trolley into the growth chamber by a manipulator arm. The load lock is accessed through a clean hood. Rough and high vacuum for the load lock, buffer chamber, and growth chamber is provided by three mechanical roughing pumps, two molecular drag pumps, one turbomolecular pump, one ion pump, and two cryopumps.

For more information, contact Dr. Cammy Abernathy: (352) 846-1087
http://www.mse.ufl.edu/~caber/

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